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The results obtained on these three samples from TGA and DSC are shown in Figures 15.25 15.36. They show the mass left and heat ow into or out from the sample as a function of temperature. The TGA results on cellulose show the presence of combined moisture in the sample under both inert and oxidative

The styrene is separated from the product mix, which also contains unreacted ethylbenzene and other impurities, by vacuum distillation The monomer can easily autopolymerize into a hard solid and is therefore inhibited from polymerization during storage by mixing in a few parts per million of a free-radical reaction inhibitor (generally t-butyl catechol) A relatively small amount of styrene is also made by the oxidation of ethyl benzene in a process introduced by Union Carbide The ethylbenzene hydroperoxide formed by oxidation is reacted with propylene to form propylene oxide and 2-phenyl ethanol The latter compound is dehydrated to obtain styrene While bulk or emulsion polymerization can also be used for the purpose, the commercial manufacture of polystyrene is mostly carried out in a solution process using a free-radical initiator The solvent, typically ethylbenzene, used at a level of 2 30%, controls the viscosity of the solution.

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The unstructured representation means that, although the mesh is Cartesian, there is no multidimensional IJK organization of cells as would be the case in a structured grid representation, so neighboring cells cannot be directly accessed When joined with SAMRAI, cubes no longer needs to decide where to re ne This, along with managing the construction of the mesh hierarchy and all of the AMR operations, is completely determined by SAMRAI Since SAMRAI and cubes both use a Cartesian mesh description of the underlying domain along with a hierarchical description of each level, they already speak the same language The decision of when and where to apply re nement is made by SAMRAI, so the algorithms in cubes that decide where to re ne are no longer necessary, which led to a number of simpli cations.

There are two main conceptual differences between the unstructured mesh generator cubes and the cut cell engine needed for structured AMR patches First, patchCubes is needed to separate the notion of the domain bounding box from the region of cut cell generation In the original cubes, these were one and the same, but for patch-based treatment the region of cut cell generation is typically a small subset of the domain bounding box The second more computationally important difference is that mesh faces between uncut cells do not need to be explicitly computed SAMR does not need an explicit representation of an uncut face; it is implicitly available on a structured mesh, and all information about it is easily computed when needed Only the cut face information needs to be supplied.

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High-impact-grade polymer used in injection-molding and extrusion is modi ed with butadiene rubber incorporated during polymerization The solvent and residual monomer in the crude resin is removed by ash evaporation or in a devolatilizing extruder (at about 225 C) Figure 29 is a schematic of the polymerization process Expandable polystyrene is extensively used in the production of foam products and extruded foam sheets These expandable beads contain a nucleating agent and a blowing agent in addition to the high-molecular-weight polystyrene resin A hydrocarbon blowing agent, typically pentane at a level of 5 8% by weight or a chloro uorocarbon (CFC) blowing agent, might be used, The latter, however, is now restricted because of its potential for depleting stratospheric ozone, and the US industry phased out the use of ozone-depleting CFCs in expanded foams in the 1980s.

This allows us to simplify cubes by re ning only the cut cells, not the uncut cells, to the level of re nement of the requested patch Large uncut cells could remain at the coarsest level in the intermediate mesh used by cubes, since the face information associated with the re nements was not needed These two simpli cations made the interface rather straightforward SAMRAI passes individual patches at a given level, and starting from the coarsest level, patchCubes tags all the cut cells in the patch bounding box until they reach the requested level Only cut cells need to be tagged because if a large coarse cell is uncut, all its children are also uncut For patches that lie on ner levels, cubes begins by using the underlying coarse representation.

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